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液固相漫反射原位池

PX-RC-DRS-A3

液固/气液固 · 低死体积 · 瞬态光谱

产品介绍

适配各主流品牌傅里叶变换红外光谱仪和紫外-可见吸收光谱仪。配备拉曼穹顶,还可用于拉曼光谱原位表征。研究对象为气液固相或液固相体系。可在常温至高温、真空至高压范围内工作(最高温度与最高压力不可同时达到,详见参数表)。其极低的内部无效体积确保了气体的平均停留时间低于2秒,是光谱动力学研究的理想选择。
液固相漫反射原位池

产品优点

  • 支持液固、气液固体系
  • 低死体积,可用于SSITKA、MES等瞬态光谱测试
  • 进气随加热台预热,避免冷气直冲催化剂
  • 热电偶直插床层测温,更贴近真实反应温度

产品参数

温度范围 常温~850℃,精度:±0.2℃
压力范围 真空~4.0MPa *
产品材质 加热台:310S不锈钢;外壳:316不锈钢(内置循环水通道)
窗片材质 红外光谱:石英+硒化锌;紫外-可见、拉曼光谱:石英
测温方式 K型热电偶,末端直接置于床层内部测温
加热方式 双加热棒对称排列,单根20V/300W(合计600W)

备注

* 最高温度与最高压力不可同时达到,高温时须相应降压。

Liquid-Solid Diffuse Reflectance In-Situ Cell

PX-RC-DRS-A3

PRODUCT INTRO

Compatible with mainstream FTIR and UV-Vis spectrometers and equipped with a Raman dome for in-situ Raman characterization, the PX-RC-DRS-A3 is designed for gas-liquid-solid and liquid-solid systems. It covers vacuum-to-high-pressure and ambient-to-high-temperature conditions with an extremely low dead volume that keeps average gas residence time below 2 seconds, ideal for spectroscopic kinetics research.

PRODUCT ADVANTAGES

  • Supports liquid-solid and gas-liquid-solid systems
  • Low dead volume — suitable for transient spectroscopies such as SSITKA and MES
  • Inlet gas is preheated by the integrated heating stage, preventing cold gas from directly contacting the catalyst
  • Thermocouple inserted directly into the catalyst bed, giving readings closer to the true reaction temperature

PRODUCT SPECIFICATIONS

Temperature Range Ambient–850 °C; accuracy ±0.2 °C
Pressure Range Vacuum–4.0 MPa *
Body Material Heating stage: 310S stainless steel; housing: 316 stainless steel (built-in water-cooling channel)
Window Material IR: Quartz + ZnSe; UV-Vis / Raman: Quartz
Temperature Sensing K-type thermocouple, tip placed directly inside the catalyst bed
Heating Method Twin heating rods in symmetric arrangement, 20 V/300 W per rod (600 W total)

NOTE

* Maximum temperature and maximum pressure cannot be reached simultaneously; reduce the working pressure accordingly at elevated temperature.