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液相全反射红外原位池

PX-RC-ATR-A2

液相原位监测 · 三款配置 · 材料可选

产品介绍

适配各品牌傅里叶变换红外光谱仪,与OPRex-ATR全反射附件联用,用于液相及液固相体系的实时原位监测。采用石英反应瓶、机械搅拌和ATR晶片组合,提供常规版、循环介质控温版和电加热夹套版。圆柱形底座及下方支承方板默认采用PEEK,可整套选用PTFE;密封垫片及垫圈默认采用全氟醚橡胶。两种控温款配加长NTC探头,实际液温在搅拌控制器上显示。
液相全反射红外原位池

产品优点

  • 三款配置:常温实验、循环介质升降温和电加热可按实验条件选择
  • 材料可选:PEEK底座和方板可整套改为PTFE,配全氟醚密封,适配不同样品体系

产品参数

常规版 单层石英反应瓶,不配主动控温部件
循环介质控温版 双层夹套石英反应瓶,夹层通循环介质;循环装置及介质由客户自配,不包含在产品内
电加热夹套版 单层石英反应瓶,配外部电加热夹套及独立温控仪
底座与支承方板 默认PEEK;选PTFE时圆柱形底座与下方方板一起更换
密封垫片与垫圈 默认全氟醚橡胶(FFKM)
循环款温度范围 -20~150℃,实际范围由循环装置、介质及实配部件允许温度共同限定
电加热款温度范围 室温~200℃,夹套控温探头位于夹套内侧并贴紧石英瓶外壁
液相温度监测 两种控温款配加长NTC热敏电阻(10K3950),从上部斜口伸入溶液,接搅拌控制器显示;不作加热闭环反馈
搅拌 机械搅拌,支持调速、正反转及定时
压力范围 真空~微正压
ATR晶片材质 硅、锗、硒化锌,按样品体系与温度条件确认
液路接口 支持连续流动进样

备注

循环款由客户的循环装置控制介质温度,电加热款由独立温控仪控制夹套温度;实际液温单独监测。瓶体接口及加长探头尺寸按配套结构确定。

Liquid-Phase Attenuated Total Reflectance In-Situ Cell

PX-RC-ATR-A2

PRODUCT INTRO

Compatible with FTIR spectrometers of all brands and used with the OPRex-ATR accessory, this cell provides real-time in-situ monitoring of liquid and liquid–solid systems. It combines a quartz reaction vessel, mechanical stirring and an ATR crystal, with standard, circulating-medium temperature-control and electric-heating-jacket versions. The cylindrical base and supporting square plate are PEEK as standard and can both be supplied in PTFE; sealing gaskets and rings are perfluoroelastomer as standard. Both temperature-control versions include an extended NTC probe, with the actual liquid temperature displayed on the stirring controller.

PRODUCT ADVANTAGES

  • Three configurations: choose ambient-temperature operation, circulating-medium heating/cooling or electric heating to suit the experiment
  • Material options: the PEEK base and square plate can both be supplied in PTFE, with perfluoroelastomer seals, to suit different sample systems

PRODUCT SPECIFICATIONS

Standard Version Single-wall quartz vessel; no active temperature-control components
Circulating-Medium Version Double-wall jacketed quartz vessel with circulating medium in the jacket; circulator and medium are customer-supplied and are not included
Electric-Heating-Jacket Version Single-wall quartz vessel with an external electric heating jacket and a separate temperature controller
Base and Supporting Square Plate PEEK as standard; when PTFE is selected, both the cylindrical base and the lower square plate are replaced
Sealing Gaskets and Rings Perfluoroelastomer (FFKM) as standard
Circulating Version Temperature Range −20 to 150 °C; actual range is limited jointly by the circulator, medium and fitted components
Electric-Heating Version Temperature Range Ambient–200 °C; the control sensor is inside the heating jacket and in close contact with the quartz vessel outer wall
Liquid Temperature Monitoring Both temperature-control versions use an extended 10K3950 NTC thermistor inserted through an upper angled port and connected to the stirring controller for display; it is not the heating-loop feedback sensor
Stirring Mechanical stirring with adjustable speed, forward/reverse rotation and timer
Pressure Range Vacuum–slight positive pressure
ATR Crystal Material Silicon, germanium or zinc selenide; selected to suit the sample system and temperature conditions
Fluidic Interface Continuous flow injection supported

NOTE

The customer’s circulator controls the medium temperature in the circulating version; a separate controller controls the heating-jacket temperature in the electric version. Actual liquid temperature is monitored separately. Vessel interfaces and extended probe dimensions are matched to the fitted assembly.